All mechanisms

Electrophilic substitution — Friedel–Crafts acylation

Year 2
AQA 3.3.10

Carbonyl & aromatic chemistry · ethanoyl chloride + AlCl₃ (catalyst) · heat under reflux, anhydrous

Reagents: ethanoyl chloride + AlCl₃ (catalyst) · Conditions: heat under reflux, anhydrous

Step 1 of 2

CCCCCCC+OCH3
  1. 1.Two electrons from the delocalised π ring attack the positively charged carbon of the acylium ion, forming a new C–C bond.
CH3COCl+AlCl3CH3CO++AlCl4

AlCl₃ removes a chloride from ethanoyl chloride: CH₃COCl + AlCl₃ → CH₃CO⁺ + AlCl₄⁻. The acylium ion CH₃CO⁺ is the electrophile.

The ring bonds to the acylium carbon, breaking aromaticity: the horseshoe (Wheland) intermediate.

Step 2 of 2

+CCCCCCHCOCH3
  1. 1.The C–H bonding pair moves back into the ring, restoring aromaticity and releasing H⁺.
H++AlCl4AlCl3+HCl

The H⁺ lost from the ring reacts with AlCl₄⁻: H⁺ + AlCl₄⁻ → AlCl₃ + HCl, regenerating the catalyst.

Aromaticity is restored and H⁺ is lost (regenerating AlCl₃): phenylethanone forms.

Product: phenylethanone

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