Chemistry

GCSE identification tests

GCSE
AQA 4.8

Flame colours, precipitates and gas tests — the whole qualitative-analysis topic on one page, with the AQA observation wording. Flip on Test yourself to drill it.

Reading mode — every observation on show.

Flame tests (metal ions)

Clean a nichrome wire in acid, dip in the sample, hold in a blue Bunsen flame. A mixture can mask colours — that's why instruments are more reliable (see below).

Ion / gasPositive result
Lithium, Li⁺crimson red
Sodium, Na⁺yellow
Potassium, K⁺lilac
Calcium, Ca²⁺orange-red
Copper, Cu²⁺green

Metal hydroxides (add sodium hydroxide)

Ion / gasPositive result
Aluminium, Al³⁺white ppt — dissolves in excess NaOH

the white ppt that redissolves — distinguishes Al³⁺ from Ca²⁺/Mg²⁺

Calcium, Ca²⁺white ppt — insoluble in excess
Magnesium, Mg²⁺white ppt — insoluble in excess
Copper(II), Cu²⁺blue ppt
Iron(II), Fe²⁺green ppt
Iron(III), Fe³⁺brown ppt

Gas tests

Ion / gasTestPositive result
Hydrogen, H₂lit splintsqueaky pop
Oxygen, O₂glowing splintrelights the splint
Carbon dioxide, CO₂bubble through limewaterlimewater turns milky/cloudy
Chlorine, Cl₂damp litmus paperbleaches it white
Ammonia, NH₃damp red litmus paperturns it blue

Negative ions (anions)

Ion / gasTestPositive result
Carbonate, CO₃²⁻add dilute acidfizzes; gas turns limewater milky (CO₂)
Sulfate, SO₄²⁻add dilute HCl, then barium chloridewhite precipitate (BaSO₄)

add HCl first to remove carbonates that would also give a ppt

Chloride, Cl⁻add dilute HNO₃, then silver nitratewhite precipitate (AgCl)
Bromide, Br⁻add dilute HNO₃, then silver nitratecream precipitate (AgBr)
Iodide, I⁻add dilute HNO₃, then silver nitrateyellow precipitate (AgI)

Instrumental methods

Machines like flame emission spectroscopy are more accurate, sensitive and rapid than flame tests, and can identify ions in a mixture. The output is a line spectrum; the pattern of lines identifies the metal ion and the intensity gives its concentration.

Drill it with flashcards

The AQA GCSE Chemistry deck tests these — and the rest of the spec — with spaced repetition.

AQA GCSE Chemistry flashcards

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